中国现代中药2017,Vol.19Issue(2):192-195,4.DOI:10.13313/j.issn.1673-4890.2017.2.006
海南砂仁脂溶性成分的GC-MS分析
GC-MS Analysis of Lipid Soluble Composition from Fruits of Amomum longiligulare
摘要
Abstract
Objective:To investigate the chemical constituents in the lipid soluble composition from the fruits of Amomum longiligulare.Methods:The petroleum ether fraction was extracted by solvent step by step and its chemical constituents were separated,determined and identified by gas chromatography-mass spectrometry combined with computer retrieval in compound databases.The relative percentage content of each compound was calculated by peak area normalization method.Results:76 compounds were separated and 56 of them were identified,which covered 68.81% of the total lipid soluble composition.The major constituents with higher relative content were hydroquinone (7.74%),Z,E-2,13-octadecadien-1-ol (6.86%),E,E-2,13-octadecadien-1-ol (5.44%),4-undecylphenol (3.71%),(Z)-9-octadecenal (3.65%),cis-vaccenic acid (3.39 %) and (E,E)-germacra-3,7 (11),9-trien-6-one (3.05 %).Conclusion:Chemical constituents of the petroleum ether fraction from the fruits of A.longiligulare were analyzed for the first time.The present study provides a chemical basis for A.longiligulare.关键词
海南砂仁/脂溶性成分/气相色谱-质谱/海南Key words
Amomum longiligulare T.L Wu/lipid soluble composition/GC-MS/Hainan引用本文复制引用
董琳,王勇,张小坡,魏娜,李友宾,张俊清,罗喻超..海南砂仁脂溶性成分的GC-MS分析[J].中国现代中药,2017,19(2):192-195,4.基金项目
海南省自然科学基金项目(20158370) (20158370)