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海南砂仁脂溶性成分的GC-MS分析

董琳 王勇 张小坡 魏娜 李友宾 张俊清 罗喻超

中国现代中药2017,Vol.19Issue(2):192-195,4.
中国现代中药2017,Vol.19Issue(2):192-195,4.DOI:10.13313/j.issn.1673-4890.2017.2.006

海南砂仁脂溶性成分的GC-MS分析

GC-MS Analysis of Lipid Soluble Composition from Fruits of Amomum longiligulare

董琳 1王勇 2张小坡 3魏娜 1李友宾 2张俊清 3罗喻超1

作者信息

  • 1. 海南医学院药学院,海南海口571199
  • 2. 海南省热带药用植物研究开发重点实验室,海南海口571199
  • 3. 海口市黎族医药重点实验室,海南海口571199
  • 折叠

摘要

Abstract

Objective:To investigate the chemical constituents in the lipid soluble composition from the fruits of Amomum longiligulare.Methods:The petroleum ether fraction was extracted by solvent step by step and its chemical constituents were separated,determined and identified by gas chromatography-mass spectrometry combined with computer retrieval in compound databases.The relative percentage content of each compound was calculated by peak area normalization method.Results:76 compounds were separated and 56 of them were identified,which covered 68.81% of the total lipid soluble composition.The major constituents with higher relative content were hydroquinone (7.74%),Z,E-2,13-octadecadien-1-ol (6.86%),E,E-2,13-octadecadien-1-ol (5.44%),4-undecylphenol (3.71%),(Z)-9-octadecenal (3.65%),cis-vaccenic acid (3.39 %) and (E,E)-germacra-3,7 (11),9-trien-6-one (3.05 %).Conclusion:Chemical constituents of the petroleum ether fraction from the fruits of A.longiligulare were analyzed for the first time.The present study provides a chemical basis for A.longiligulare.

关键词

海南砂仁/脂溶性成分/气相色谱-质谱/海南

Key words

Amomum longiligulare T.L Wu/lipid soluble composition/GC-MS/Hainan

引用本文复制引用

董琳,王勇,张小坡,魏娜,李友宾,张俊清,罗喻超..海南砂仁脂溶性成分的GC-MS分析[J].中国现代中药,2017,19(2):192-195,4.

基金项目

海南省自然科学基金项目(20158370) (20158370)

中国现代中药

OACSTPCD

1673-4890

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