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微波消解法测定高氯废水的COD探讨

冯栩 鲍晋 曹潜 刘涛 刘恒 梁婧华 夏丽娟 杨阳

西华大学学报(自然科学版)2017,Vol.36Issue(2):91-95,5.
西华大学学报(自然科学版)2017,Vol.36Issue(2):91-95,5.DOI:10.3969/j.issn.1673-159X.2017.02.018

微波消解法测定高氯废水的COD探讨

Research on Testing of COD in Wastewater Containing High Chlorine Based on Microwave Digestion Method

冯栩 1鲍晋 2曹潜 1刘涛 1刘恒 1梁婧华 1夏丽娟 1杨阳1

作者信息

  • 1. 西华大学食品与生物工程学院,四川成都610039
  • 2. 川庆钻探工程有限公司井下作业公司,四川成都610051
  • 折叠

摘要

Abstract

Chlorides in the wastewater with high concentration seriously interrupts the determination of chemical oxygen demand (COD).Microwave digestion method was used to test COD of wastewater with high chlorine.The experiment results show that for this method,the effect of C1-is weaker than that by traditional potassium dichromate method.As the concentration of C1-is between 0 ~ 30 000 mg/L and COD≤500 mg/L,a certain amount of mercuric sulfate would be added during the COD test,and fractional error of test result is less than ± 5%,which was in the scope of national standard.When the COD of shell gas fracturing flow-back fluid was tested,the effect of C1-on the COD test would be eliminated by using microwave digestion method and the test results was accurate and reliable.

关键词

微波消解法/高氯废水/COD

Key words

microwave digestion method/high chlorine containing wastewater/COD

分类

资源环境

引用本文复制引用

冯栩,鲍晋,曹潜,刘涛,刘恒,梁婧华,夏丽娟,杨阳..微波消解法测定高氯废水的COD探讨[J].西华大学学报(自然科学版),2017,36(2):91-95,5.

基金项目

西华大学重点科研基金项目(z1220409、Z1520526) (z1220409、Z1520526)

四川省教育厅项目(14ZB0125). (14ZB0125)

西华大学学报(自然科学版)

OACSTPCD

1673-159X

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