纺织高校基础科学学报2017，Vol.30Issue(1)：91-95,5.DOI:10.13338/j.issn.1006-8341.2017.01.016
水热法制备WO3-MCM-41及其催化性能
Characterization and catalytic performance of synthesized WO3-MCM-41 by hydrothermal method
摘要
Abstract
WO3-MCM-41 was synthesized from hydrothermal method.The composition and size of the WO3-MCM-41 were characterized through X-ray diffraction (XRD),scanning electron microscope (SEM) and X-ray photoelectron spectroscopy (XPS).The results show that the WO3-MCM-41 is uniform round particles about 300nm and the WO3 is well-distributed on MCM-41.The catalytic activity was investigated by cyclohexanone to adipic acid using H2O2.The results show that when Si/W mole ratio of 1 ∶ 0.6,catalyst amount 2.5 g,30％H2O2 40mL,the yield of adipic acid is up to 51.6％.关键词
水热法/WO3-MCM-41/催化活性Key words
hydrothermal method/WO3-MCM-41/catalytic activity分类
化学化工引用本文复制引用
李红,王晓燕,张江龙..水热法制备WO3-MCM-41及其催化性能[J].纺织高校基础科学学报,2017,30(1):91-95,5.基金项目
陕西省教育厅专项科研计划项目(2010JK574) （2010JK574）
西安工程大学博士启动项目(BS0917) （BS0917）
