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低含盐量月桂酰胺丙基甜菜碱的合成及性能研究

鞠洪斌 耿涛 姜亚洁 王亚魁

印染助剂2017,Vol.34Issue(4):12-15,4.
印染助剂2017,Vol.34Issue(4):12-15,4.

低含盐量月桂酰胺丙基甜菜碱的合成及性能研究

Synthesis and properties of lauroylamidopropyl betaine with low salt content

鞠洪斌 1耿涛 1姜亚洁 1王亚魁1

作者信息

  • 1. 中国日用化学工业研究院,山西太原 030001
  • 折叠

摘要

Abstract

Lauroylamidopropyl betaine with low salt content was synthesized from lauric acid, N,N- di-methyl- 1,3- diaminopropane and sodium chloroacetate by two- steps, amidazation and quaternization. The structure and main properties of products were determined by FTIR and 1HNMR. The results showed that the contents of active substance reached 82.00% and NaCl mass fraction decreased significantly. When the active substance solution was 30%, the mass fraction of NaCl was only about 1.79%, and the mass fraction of unre-acted amine was 0.30%. At the same time, the lowest surface tension of solutions was 26.76 mN/m, cmc was 3.65 mmol/L and viscosity was 88.81 mPa·s.

关键词

月桂酰胺丙基甜菜碱/两步反应/低盐质量分数/表面张力

Key words

lauroylamidopropyl betaine/two- steps/low salt content/surface tensions

分类

化学化工

引用本文复制引用

鞠洪斌,耿涛,姜亚洁,王亚魁..低含盐量月桂酰胺丙基甜菜碱的合成及性能研究[J].印染助剂,2017,34(4):12-15,4.

基金项目

"十二五"国家科技支撑计划项目(2014BAE03B00) (2014BAE03B00)

山西省科技攻关项目(20130321019-02) (20130321019-02)

山西省专利转化与推广项目(20051009) (20051009)

印染助剂

OA北大核心CSTPCD

1004-0439

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