中国药业2017,Vol.26Issue(8):12-16,5.DOI:10.3969/j.issn.1006-4931.2017.08.004
清金固本胶囊质量控制方法研究
Quality Control of Qingjinguben Capsule
摘要
Abstract
Objective To control the quality of Qingjinguben Capsule. Methods TLC method was used to identify Scutellariae Radix, Platycodonis Radix,Poria,Saposhnikoviae Radix,Codonopsis. The content of baicalin was determined by HPLC. Results The chromato-graphic spots were clear with good separation,the chromatogram for identification by TLC was distinct and highly specific. The linear range was 4. 1-32. 8 μg/ml(r=0. 9999),the average recovery rate was 95. 85%,RSD was 0. 71%(n=6). Conclusion The method can provide reference for the establishment of quality standard of Qingjinguben Capsule.关键词
清金固本胶囊/薄层色谱鉴别/高效液相色谱法/黄芩苷/含量测定/质量控制Key words
Qingjinguben Capsule/TLC/HPLC/baicalin/content determination/quality contorl分类
医药卫生引用本文复制引用
李玎,李娜,张敏婕,陈萍..清金固本胶囊质量控制方法研究[J].中国药业,2017,26(8):12-16,5.基金项目
陕西省自然科学基础研究计划项目[ 2012JM4053 ]. ()