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FPD气相色谱法测定液晶材料中微量有机膦杂质

霍学兵 韩锦伟 张鹏 耿红超 葛强 丁兴立

液晶与显示2017,Vol.32Issue(5):357-360,4.
液晶与显示2017,Vol.32Issue(5):357-360,4.DOI:10.3788/YJYXS20173205.0357

FPD气相色谱法测定液晶材料中微量有机膦杂质

Determination of organic phosphorus impurities in liquid crystal materials by FPD gas chromatography

霍学兵 1韩锦伟 1张鹏 1耿红超 1葛强 1丁兴立1

作者信息

  • 1. 阜阳欣奕华材料科技有限公司,安徽 阜阳 236000
  • 折叠

摘要

Abstract

A FPD-GC method for determination of organic phosphorus impurities in liquid crystal material was established.The method with good reproducibility can be applied to simultaneous determination of triphenylphosphine and triphenylphosphine oxide.The relative standard deviations (RSD, n =5) of triphenylphosphine oxide and triphenylphosphine were 4.4% and 5.6%.The recoveries ranged from 80% to 110%.The experiment has a good guiding significance to the establishment of the analytical method in the process of industrialization.

关键词

液晶材料/有机膦杂质/FPD

Key words

liquid crystal material/organic phosphorus impurities/FPD

分类

数理科学

引用本文复制引用

霍学兵,韩锦伟,张鹏,耿红超,葛强,丁兴立..FPD气相色谱法测定液晶材料中微量有机膦杂质[J].液晶与显示,2017,32(5):357-360,4.

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