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功能化二硫化钼/聚酰胺复合材料的制备及性能研究

梁霄 陈鹏鹏 周艺峰 聂王焰

安徽大学学报(自然科学版)2017,Vol.41Issue(2):84-91,8.
安徽大学学报(自然科学版)2017,Vol.41Issue(2):84-91,8.DOI:10.3969/j.issn.1000-2162.2017.02.012

功能化二硫化钼/聚酰胺复合材料的制备及性能研究

Preparation and properties of functionalized MoS2/polyamide-6 composites

梁霄 1陈鹏鹏 1周艺峰 1聂王焰1

作者信息

  • 1. 安徽大学化学化工学院,安徽省绿色高分子材料重点实验室,安徽合肥230601
  • 折叠

摘要

Abstract

Molybdenum disulfide (MoS2) was exfoliated by Li+ intercalation method.The exfoliated MoS2 was functionalized with cysteamine to obtain MoS2-NH2.The PA-g MoS2 was synthesized via ring-opening polymerization using ε-caprolactam initiated by MoS2-NH2 and characterized by FT-IR,XRD and XPS.The functionalized MoS2/polyamide composites (MPA) were fabricated via a simple melt compounding method.The thermal and mechanical properties of MPA were characterized by DSC,TGA and DMTA,which indicated that the thermal stability of PA was improved apparently with the increase of PA-g-MoS2,while the mechanical property was decreased.

关键词

二硫化钼/ε-己内酰胺/开环聚合/复合材料

Key words

MoS2/ε-caprolactam/ring-opening polymerization/composites

分类

化学化工

引用本文复制引用

梁霄,陈鹏鹏,周艺峰,聂王焰..功能化二硫化钼/聚酰胺复合材料的制备及性能研究[J].安徽大学学报(自然科学版),2017,41(2):84-91,8.

基金项目

国家自然科学基金资助项目(51403003) (51403003)

安徽大学学报(自然科学版)

OA北大核心CSTPCD

1000-2162

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