食品工业科技2017，Vol.38Issue(7)：293-294,310,3.DOI:10.13386/j.issn1002-0306.2017.07.048
石菖蒲中高纯度β-细辛醚和α-细辛醚的制备
Preparation of high purity β-asarone and α-asarone from Acorus tatarinowii Schott
摘要
Abstract
To establish a method for preparation of high purity β-asarone and α-asarone from Acorus tatarinowii Schott by high pressure semi-preparative liquid chromatography,its volatile oil was prepared from Acorus tatarinowii Schott,and a semi-preparative high performance liquid chromatography was used to refine and purifyβ-asarone and α-asarone with a solvent composed of methanol and water(65:35,v/v).The structures of product were identified by EI-MS,1H-NMR and13 C-NMR,and their purities reached 99.43％ and 99.08％,respectively.The method is easily operated,with high purity and preparation amount.It is suitable for high purityβ-asarone and α-asarone reference material preparation from Acorus tatarinowii Schott.关键词
石菖蒲/高压半制备液相色谱法/β-细辛醚/α-细辛醚/纯化Key words
Acorus tatarinowii Schott/high pressure semi-preparative liquid chromatography/β-asarone/α-asarone/purification分类
轻工纺织引用本文复制引用
裘纪莹,赵双枝,赵玉忠,陈蕾蕾,王同燕,王未名..石菖蒲中高纯度β-细辛醚和α-细辛醚的制备[J].食品工业科技,2017,38(7):293-294,310,3.基金项目
山东省自然科学基金三院联合基金项目(ZR2014YL020) （ZR2014YL020）
山东省农业科学院青年科研基金项目(2014QNM47) （2014QNM47）
泰山学者建设工程专项. （）
