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紫外分光光度法测定恩诺沙星微囊含量方法的建立

苏晓晴 徐之勇 张李琦 郑明学 戴浩楠 史晨婕 白瑞 席柔 贡鑫 张黎

山西农业大学学报(自然科学版)2017,Vol.37Issue(4):258-262,5.
山西农业大学学报(自然科学版)2017,Vol.37Issue(4):258-262,5.

紫外分光光度法测定恩诺沙星微囊含量方法的建立

Determination of enrofloxacin gelatin microcapsules content by UV spectrophotometry

苏晓晴 1徐之勇 1张李琦 1郑明学 1戴浩楠 1史晨婕 1白瑞 1席柔 1贡鑫 1张黎1

作者信息

  • 1. 山西农业大学动物科技学院,山西太谷030801
  • 折叠

摘要

Abstract

[Objective]The aim of this paper was to establish an UV spectrophotometry method for the determination of enrofloxacin content in enrofloxacin gelatin microcapsules.[Methods]The specificity,linearity,accuracy and precision were tested in this study.[Results]A good linearity was obtained for enrofloxacin in the range of 2~16 μg/mL and the standard curvilinear equation was A=0.103 0C-0.028 0(r=0.998 8).The relative standard deviation(RSD) of precision test was 0.00%、0.14%、0.11%(n=3),the average recovery rate was 101.53% 、98.03% 、98.07%(n=3)and its RSD was 0.25% 、0.05%、0.00%(n=3),respectively.[Conclusion] The specificity,linearity,precision and recovery rate were all consistent with the request.The method could be used for the quality control of enrofloxacin gelatin microcapsules.

关键词

恩诺沙星/明胶微囊/紫外分光光度法

Key words

UV spectrophotometry/Enrofloxacin/Gelatin microcapsules

分类

农业科技

引用本文复制引用

苏晓晴,徐之勇,张李琦,郑明学,戴浩楠,史晨婕,白瑞,席柔,贡鑫,张黎..紫外分光光度法测定恩诺沙星微囊含量方法的建立[J].山西农业大学学报(自然科学版),2017,37(4):258-262,5.

基金项目

山西省现代农业鸡产业技术体系项目(2016-11-03) (2016-11-03)

山西农业大学学报(自然科学版)

OA北大核心CSTPCD

1671-8151

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