杭州师范大学学报(自然科学版)2017,Vol.16Issue(3):230-235,272,7.DOI:10.3969/j.issn.1674-232X.2017.03.002
2,3-2H-2-(2-(4-苯基哌嗪-1-基)喹啉-3-基)-4-苯基-1,5-苯并的合成与表征
Synthesis and Characterization of 2,3-Dihydro-2-(2-(4-Phenylpiperazin-1-yl)quinolin-3-yl)-4-Phenyl-1,5-Benzothiazepine
摘要
Abstract
C34H30N4S with quinoline and piperazine was synthesized.Its crystal structure was determined as triclinic system by elemental analysis,IR,1H NMR,MS and X-ray crystallographic analysis.The space group is P-1.The seven membered heterocyclic ring of the thiazepino moiety adopts a twist-boat conformation and the piperazino moiety adopts a chair conformation.The crystal structure is stabilized because of the interactions of C-H…N and C-H…S.关键词
苯并/喹啉/4-苯基哌嗪/晶体结构Key words
benzothiazepine/quinoline/4-phenylpiperazine/crystal structure分类
化学化工引用本文复制引用
杨鹏,戚璐璐,许芯宁,刘方明..2,3-2H-2-(2-(4-苯基哌嗪-1-基)喹啉-3-基)-4-苯基-1,5-苯并的合成与表征[J].杭州师范大学学报(自然科学版),2017,16(3):230-235,272,7.基金项目
国家自然科学基金项目(29702007,20162004) (29702007,20162004)
浙江省自然科学基金项目(B02021901). (B02021901)