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核桃壳粉液化产物大孔泡沫炭的制备研究

万永坤 刘守庆 赵建蓉 黄元波 郑志锋 李雪梅

西南林业大学学报2017,Vol.37Issue(3):192-198,7.
西南林业大学学报2017,Vol.37Issue(3):192-198,7.DOI:10.11929/j.issn.2095-1914.2017.03.031

核桃壳粉液化产物大孔泡沫炭的制备研究

The Preparation of Carbon Foam with Macropores Structure from the Phenolated Walnut Shell Powder

万永坤 1刘守庆 1赵建蓉 1黄元波 2郑志锋 3李雪梅2

作者信息

  • 1. 西南林业大学理学院, 云南 昆明650224
  • 2. 西南林业大学材料工程学院, 云南 昆明650224
  • 3. 西南林业大学西南山地森林资源保育与利用省部共建教育部重点实验室, 云南 昆明650224
  • 折叠

摘要

Abstract

Foamable phenol resin of liquefied products of walnut ( Juglans regia) shell powder was prepared, and then macroporous carbon foam was obtained by foaming method. In this study, effect of foaming condition on the microstructure, bulk density and compressive strength of the carbon foam were mainly investigated. Results showed that the liquefied product resin had the foaming performance with formaldehyde and it could be used to pre-pare the carbon foam. The optimum conditions were obtained through image analysis of the bulk density, compressive strength and microstructure. The dosage of curing agent, foaming agent and surfactant were 5%-6%, 2%-3% and 8% respectively. The experiment was conducted which the dosage of curing agent, foaming agent and surfactant were 5%, 2% and 8%respectively, and macropore carbon foam was obtained which it had high opening porosity, uniform pore distribution, bulk density of 0. 34 g/cm3, compressive strength of 6. 7 MPa and average pore size of 40-70μm.

关键词

核桃壳/泡沫炭/液化/树脂化/发泡材料

Key words

walnut shell/carbon foam/liquefaction/resinification/foaming material

分类

农业科技

引用本文复制引用

万永坤,刘守庆,赵建蓉,黄元波,郑志锋,李雪梅..核桃壳粉液化产物大孔泡沫炭的制备研究[J].西南林业大学学报,2017,37(3):192-198,7.

基金项目

西南林业大学大学生科技创新项目 (15104) 资助 (15104)

国家自然科学基金项目 (31160147) 资助 (31160147)

云南省应用基础研究重点项目 (2014FA034) 资助. (2014FA034)

西南林业大学学报

OA北大核心CSTPCD

2095-1914

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