金刚石与磨料磨具工程2017，Vol.37Issue(1)：43-46,4.DOI:10.13394/j.cnki.jgszz.2017.1.0008
SPS烧结诱发自蔓延反应制备Ti3SiC2-金刚石复合材料
Fabricating Ti3SiC2-diamond composites by spark plasma sintering induced self-propagation reaction
摘要
Abstract
Ti3SiC2-diamond composites were fabricated by spark plasma sintering induced selfpropagation reaction with 3Ti/Si/2C powders as bonder.The effect of holding time on the phase composition and microstructure of composites were studied.The result shows that Ti3 SiC2 phase is formed when heated at 1170 ℃,whose main phases are Ti3SiC2,Ti5Si3 and TiC.It is also found that Ti3SiC2 content in the sample obtained at 1500 ℃ is higher with fully reacted raw materials.The main phase of the sample containing 10wt％0 diamond is TiaSiC2 and TiC.Additionally,small amounts of Si,SiC and diamond are also obtained.Ti3 SiC2 content in the sample with holding time of 1 min is higher,whose grains is lathe-structured and bonds well with diamond.Ti3SiC2 content in the sample with holding time of 5 min is lower,mainly composed of many TiC particles.In addition,the diamond is seriously graphitized,forming thick transition layer.关键词
复合物构成和结构/显微形貌/石墨化/过渡层Key words
composition and structure of composites/micro topography/graphitize/transition layer分类
化学化工引用本文复制引用
张旺玺,夏涛,罗伟,梁宝岩..SPS烧结诱发自蔓延反应制备Ti3SiC2-金刚石复合材料[J].金刚石与磨料磨具工程,2017,37(1):43-46,4.基金项目
河南省高等学校重点科研项目(17A430034) （17A430034）
河南省高校创新团队项目(15IRTSTHN004) （15IRTSTHN004）
河南省省院科技合作项目(142106000193) （142106000193）
河南省教育厅自然科学研究计划项目资助(14A430007) （14A430007）
河南省科技开放合作项目(142106000051) （142106000051）
郑州市国际科技合作与交流项目(153PGJHZ209) （153PGJHZ209）
郑州市人才引育项目(141PRCYY514). （141PRCYY514）
