中成药2017，Vol.39Issue(3)：540-543,4.DOI:10.3969/j.issn.1001-1528.2017.03.020
黑果菝葜根茎化学成分的研究
Chemical constituents from the rhizomas of Smilax glauco-china
摘要
Abstract
AIM To study the chemical constituents from the rhizomas of Smilax glauco-china Warb.METHODS The n-butanol fraction of ethanol extract of S.glauco-china was isolated and purified by silica,Sephadex LH-20 and semi-preparative column,then the structures of obtained compounds were identified by physicochemical properties and spectral data.RESULTS Ten compounds were isolated and identified as phenethanol-β-D-gentiobioside (1),2-phenylethyl-O-β-D-xylopyranosyl-(1 →6)-β-D-glucopyranoside (2),phenylethyl D-rutinoside (3),phenylethyl β-D-glucoside (4),hydrangeifolin Ⅰ (5),icariside D1 (6),calophymembranside B (7),2-hydroxyphenol-1-O-β-D-glucopyranosyl-(6 → 1)-α-L-rhamnopyranoside (8),β-sitosterol (9),daucosterol (10).CONCLUSION All the compounds are isolated from this plant for the first time.关键词
黑果菝葜/根茎/化学成分/分离鉴定Key words
Smilax glauco-china Warb/rhizomas/chemical constituents/isolation and identification分类
医药卫生引用本文复制引用
刘敏,郑小花,朱根华,黄慧莲,舒积成,邵峰,刘荣华..黑果菝葜根茎化学成分的研究[J].中成药,2017,39(3):540-543,4.基金项目
国家自然科学基金项目(31370376,81360628) （31370376,81360628）
江西省科技厅重点研发计划(20151BBG70141) （20151BBG70141）
