硅酸盐通报2017，Vol.36Issue(5)：1470-1479,10.
溶胶-凝胶二氧化硅微球粒径的响应曲面法优化研究
Particle Size of Sol-gel-silica Microspheres by Response Surface Methodology
摘要
Abstract
The particle size of silica microspheres synthesized by sol-gel method was optimized by response surface method.The effect of single factor on particle size was studied and discussed.Based on the experimental conditions selected by the single factor experiment, the experiment was designed according to the response surface method.The data were analyzed by quadratic regression and variance analysis and the insignificant terms are deleted and refitted to make the model reflect the actual situation better.Based on the fitted model, the influence of the interaction was analyzed.The suitable range of sol-gel method and the synthesis conditions of specific particle size were predicted.It is found that the error value is within 100 nm, which can provide a good reference for the later researchers.关键词
响应曲面法/溶胶凝胶法/二氧化硅微球/粒径Key words
response surface methodology/sol gel/silica microsphere/particle size分类
化学化工引用本文复制引用
张家豪,师超,邵亚薇,王艳秋,刘斌,孟国哲..溶胶-凝胶二氧化硅微球粒径的响应曲面法优化研究[J].硅酸盐通报,2017,36(5):1470-1479,10.基金项目
国家国际科技合作计划项目(2014DFR50560) （2014DFR50560）
科技部国家重点研发计划(2016YFB0300604) （2016YFB0300604）
中央高校基本科研业务费专项资金(HEUCFZ1502) （HEUCFZ1502）
