材料科学与工程学报2017，Vol.35Issue(3)：374-379,6.DOI:10.14136/j.cnki.issn1673-2812.2017.03.006
高可见光活性磁性催化剂ZnO/ZnFe2O4/石墨烯的制备与表征
Preparation and Characterization of High Visible Light Photocatalytic Activity of Magnetic Catalyst ZnO/ZnFe2O4/graphene
毛洪凯 1罗驹华 2颜柱 1申盼2
作者信息
- 1. 江苏大学材料科学与工程学院,江苏镇江212000
- 2. 盐城工学院材料工程学院,江苏盐城224051
- 折叠
摘要
Abstract
ZnO/ZnFe2O4 nanoparticles were synthesised by one-step hydrothermal method using zinc nitrate and ferrous sulfate as raw materials.Then ZnO/ZnFe2O4/graphene was prepared by reduction of graphene oxide with hydrazine hydrate.The structure of the catalyst was analyzed by means of XRD (X-ray Diffraction),FESEM (Field Emission Scanning Electron Microscopy),TEM (Transmission Electron Nicroscope),FT-IR(Fourier Transform Infrared Spectoscopy) and other characterization methods.Methylene blue was used as a target to evaluate the photocatalytic activity of the composite catalysts under visible light irradiation.The results show that when the content of graphene is 3％,the photocatalytic activity of the samples is highest and the degradation rate of methylene blue solution reached 98％ in 60min under the irradiation of visible light.The composite catalyst has good stability and can be easily recovered by the external magnetic field because of the existence of ZnFe2 O4.关键词
石墨烯/ZnO/ZnFe2 O4/磁性催化剂/可见光催化性能Key words
graphene/ZnO/ZnFe2O4/magnetic catalyst/visible light photocatalytic activity分类
通用工业技术引用本文复制引用
毛洪凯,罗驹华,颜柱,申盼..高可见光活性磁性催化剂ZnO/ZnFe2O4/石墨烯的制备与表征[J].材料科学与工程学报,2017,35(3):374-379,6.
