烟草科技2017，Vol.50Issue(6)：40-46,7.
HS-GC/MS法测定烟用水基胶中挥发性有机物
Determination of volatile compounds in water-based cigarette adhesives by headspace-gas chromatography/mass spectrometry
摘要
Abstract
In order to establish a general method to determine the volatile compounds in water-based cigarette adhesives, a headspace-gas chromatography/mass spectrometry (HS-GC/MS) method for determining 18 volatile compounds in water-based cigarette adhesives was established. The method used 10 mL water as the matrix correction agent, and adopting the static headspace sampling to quantify with an internal standard. The results showed that: 1) The volatile compounds were separated effectively within 26 min. All the volatile compounds had a good linear relationship (R2>0.999). The recoveries of 18 volatile compounds were in the range of 80.4%-127.8% at three spike levels with relative standard deviations no more than 7.9% . The LODs of 18 volatile compounds ranged from 0.004 to 6.932 mg/kg. This method is convenient, environment-friendly, universal and of high throughput, it is suitable for determining the volatile compounds in water-based adhesives.关键词
顶空-气相色谱/质谱联用(HS-GC/MS)/挥发性有机物/水基胶Key words
Headspace-gas chromatography/mass spectrometry(HS-GC/MS)/Volatile compound/Water-based adhesive分类
轻工纺织引用本文复制引用
刘珊珊,唐纲岭,陈晓,李倩,骆震,赵冰,刘岩顺,李中皓,柯玮,边照阳,杨飞,范子彦,王颖,邓惠敏..HS-GC/MS法测定烟用水基胶中挥发性有机物[J].烟草科技,2017,50(6):40-46,7.基金项目
国家烟草质量监督检验中心科技项目"烟用水基胶中挥发性成分的测定 顶空-气相色谱/质谱联用法"(562015CA0100) （562015CA0100）
河南中烟工业有限责任公司科技创 新 项目"烟用水基胶中部分物质分析方法研究"(ZW2015007). （ZW2015007）
