中成药2017,Vol.39Issue(7):1419-1422,4.DOI:10.3969/j.issn.1001-1528.2017.07.020
赤小豆化学成分的研究
Chemical constituents from Vigna umbellate
摘要
Abstract
AIM To study the chemical constituents from Vigna umbellata Ohwi et Ohashi.METHODS The ethyl acetate fraction of 80% ethanol extract from V.umbellata was isolated and purified by silica,Sephadex LH-20 and ODS column,then the structures of obtained compounds were identified by spectral data and physicochemical properties.RESULTS Twelve compounds were isolated and elucidated as (+) catechin (1),(-) epicatechin (2),3-furanmethanol-β-D-glucopyranoside (3),myricetin-3-O-β-D-glucopyranoside (4),quercetin7-O-β-D-glucopyranoside (5),(+) catechin-3-O-β-D-glucopyranoside (6),(+) catechin-5-O-β-D-glucopyranoside (7),quercetin-3 '-O-α-L-rhamnoside (8),(±) dihydroquercetin (9),quercetin (10),ethyl gallate (11),propanediol (12).CONCLUSION All the compounds are isolated from V.umbellata for the first time,and compounds 4,8,9,11,12 are first obtained from genus Vigna.关键词
赤小豆/化学成分/分离鉴定Key words
Vigna umbellata Ohwi et Ohashi/chemical constituents/isolation and identification分类
医药卫生引用本文复制引用
陈俏,刘晓月,石亚囡,曹佳,张婷婷,许枬..赤小豆化学成分的研究[J].中成药,2017,39(7):1419-1422,4.基金项目
2015年国家公益性行业专项项目(201507004-03) (201507004-03)