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赤小豆化学成分的研究

陈俏 刘晓月 石亚囡 曹佳 张婷婷 许枬

中成药2017,Vol.39Issue(7):1419-1422,4.
中成药2017,Vol.39Issue(7):1419-1422,4.DOI:10.3969/j.issn.1001-1528.2017.07.020

赤小豆化学成分的研究

Chemical constituents from Vigna umbellate

陈俏 1刘晓月 1石亚囡 2曹佳 1张婷婷 1许枬1

作者信息

  • 1. 辽宁中医药大学药学院,辽宁大连116600
  • 2. 大连市药品检验所,辽宁大连116021
  • 折叠

摘要

Abstract

AIM To study the chemical constituents from Vigna umbellata Ohwi et Ohashi.METHODS The ethyl acetate fraction of 80% ethanol extract from V.umbellata was isolated and purified by silica,Sephadex LH-20 and ODS column,then the structures of obtained compounds were identified by spectral data and physicochemical properties.RESULTS Twelve compounds were isolated and elucidated as (+) catechin (1),(-) epicatechin (2),3-furanmethanol-β-D-glucopyranoside (3),myricetin-3-O-β-D-glucopyranoside (4),quercetin7-O-β-D-glucopyranoside (5),(+) catechin-3-O-β-D-glucopyranoside (6),(+) catechin-5-O-β-D-glucopyranoside (7),quercetin-3 '-O-α-L-rhamnoside (8),(±) dihydroquercetin (9),quercetin (10),ethyl gallate (11),propanediol (12).CONCLUSION All the compounds are isolated from V.umbellata for the first time,and compounds 4,8,9,11,12 are first obtained from genus Vigna.

关键词

赤小豆/化学成分/分离鉴定

Key words

Vigna umbellata Ohwi et Ohashi/chemical constituents/isolation and identification

分类

医药卫生

引用本文复制引用

陈俏,刘晓月,石亚囡,曹佳,张婷婷,许枬..赤小豆化学成分的研究[J].中成药,2017,39(7):1419-1422,4.

基金项目

2015年国家公益性行业专项项目(201507004-03) (201507004-03)

中成药

OA北大核心CSCDCSTPCD

1001-1528

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