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半夏糖浆中4种有机酸的含量测定

任华忠

中药材2017,Vol.40Issue(2):384-386,3.
中药材2017,Vol.40Issue(2):384-386,3.DOI:10.13863/j.issn1001-4454.2017.02.029

半夏糖浆中4种有机酸的含量测定

The HPLC Simultaneous Detection of Four Organic Acid in Banxia Syrup

任华忠1

作者信息

  • 1. 乐山职业技术学院,四川乐山614000
  • 折叠

摘要

Abstract

Objective:To study the HPLC simultaneous detection of tartaric acid,malic acid,citric acid,and succinic acid in Banxia syrup.Methods:The analysis was carried out by Phenomenex C1s,and eluted with mobile phase containing of 0.01 mol/L NH4 H2 PO4-H3PO4 (pH =2.9),with the injection of 20 μL,the flow rate was 1.0 mL/min,the wavelength was 210 nm,and the column temperature was 30 ℃.The content of four organic acid had been detected.Results:The precision,stability,repeatability and recovery rate of this method were good.There were little difference in the contents of tartaric acid,malic acid,citric acid and succinic acid from different companies.Conclusion:This method can be a reference for quality control of Banxia syrup.

关键词

半夏糖浆/有机酸/HPLC

Key words

Banxia syrup/Organic acids/HPLC

分类

医药卫生

引用本文复制引用

任华忠..半夏糖浆中4种有机酸的含量测定[J].中药材,2017,40(2):384-386,3.

中药材

OA北大核心CSTPCD

1001-4454

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