中国药房2017，Vol.28Issue(21)：2992-2994,3.DOI:10.6039/j.issn.1001-0408.2017.21.31
GC-MS法分析红木香药材根和果实中的挥发油成分
Analysis of Volatile Oil from Roots and Fruits of Kadsura longipedunculata by GC-MS
摘要
Abstract
OBJECTIVE:To analyze volatile oil from the roots and fruits of Kadsura longipedunculata. METHODS:GC-MS method was adopted. The determination was performed on HP-5MS quartz capillary column with nitrogen as carrier gas at the flow rate of 0.9 mL/min. The temperature of sample inlet was 250 ℃,the initial temperature of column was set at 50 ℃(temperature programming). The column pressure was 80 kPa;the ratio of split sampling was 40 : 1. The sample size was 1.0 μL. Mass chroma-tography was as follows:electron bombardment ion source as ion source;electron energy of 70 eV;inlet temperature was 230 ℃;scanning range of m/z 40-400,scanning interval time of 1.0 s. RESULTS:Totally 43 chromatographic peaks were detected in vola-tile oil from the roots of K. longipedunculata,and 24 peaks were identified,accounting for 91.5%;main components were sesqui-terpenes and monoterpenoids,among which the relative contents of (+)-delta-cadinene,γ-cadinene and isovalencene were in high level. Totally 52 chromatographic peaks were detected in volatile oil from the fruits of K. longipedunculata,and 36 peaks were iden-tified,accounting for 82.2%;main components were sesquiterpenes and monoterpenoids,among which relative contents of caroph-yllene,γ-cadinene and valencene were in high level. CONCLUSIONS:The study basically confirm main volatile components in volatile oil from the roots and fruits of K. longipedunculata,and the roots and fruits of K. longipedunculata have significant differ-ence.关键词
红木香/挥发油/气相色谱-质谱联用法Key words
Kadsura longipedunculata/Volatile oil/GC-MS分类
医药卫生引用本文复制引用
姜泽静,黄泽豪..GC-MS法分析红木香药材根和果实中的挥发油成分[J].中国药房,2017,28(21):2992-2994,3.基金项目
国家中医药管理局中医药行业科研专项项目(No.201407002) （No.201407002）
