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单分散银纳米粒子的制备与表征

邢世雄 王建宇 董春法

信阳师范学院学报(自然科学版)2017,Vol.30Issue(3):440-444,5.
信阳师范学院学报(自然科学版)2017,Vol.30Issue(3):440-444,5.DOI:10.3969/j.issn.1003-0972.2017.03.020

单分散银纳米粒子的制备与表征

Synthesis and Characterion of Monodisperse Silver Nanoparticles

邢世雄 1王建宇 1董春法2

作者信息

  • 1. 黄冈师范学院 交通学院,湖北 黄冈 438000
  • 2. 湖北理工学院 机电工程学院,湖北 黄石 435003
  • 折叠

摘要

Abstract

Monodispersed silver nanoparticles were obtained by a simple route in water with PVP as the capping agents, hydrazine hydrate as the reducing agents, silver nitrate solution as the silver source.The characteriztion of as-synthesized silver nanoparticles were studied by the transmission electron microscopy, UV-vis spectuam, X-ray powder diffraction and laser particle size analyzer.The results indicated that the obtained silver nanoparticles were small with the narrowly distribution.The concentration of silver nitrate, the consumption of PVP and hydrazine hydrate played the important roles in the size and morphology of silver nanoparticles.Smallest silver naopartilces were obtained when the consumption of PVP and hydrazine hydrate was 0.2 g and 0.1 g,respectively, and the concentration of silver nitrate was 150 mg/L.

关键词

聚乙烯吡咯烷酮/纳米银/还原法/纳米材料

Key words

PVP/silver nanoparticles/reduction method/nano materials

分类

通用工业技术

引用本文复制引用

邢世雄,王建宇,董春法..单分散银纳米粒子的制备与表征[J].信阳师范学院学报(自然科学版),2017,30(3):440-444,5.

基金项目

国家自然科学基金项目(51405146) (51405146)

湖北省教育厅科研计划项目(Q20164506) (Q20164506)

信阳师范学院学报(自然科学版)

OA北大核心CSTPCD

1003-0972

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