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六水合三氯化铁中亚铁的检测方法探讨

白晓光 王正达 邬旭东 段书芬 刘爱华 程晓

中国药业2017,Vol.26Issue(16):29-31,3.
中国药业2017,Vol.26Issue(16):29-31,3.DOI:10.3969/j.issn.1006-4931.2017.16.009

六水合三氯化铁中亚铁的检测方法探讨

Determination of Ferrous Iron in Ferric Chloride Hexahydrate

白晓光 1王正达 1邬旭东 1段书芬 1刘爱华 1程晓2

作者信息

  • 1. 上海拱极化学有限公司,上海 201302
  • 2. 青岛国风药业股份有限公司,山东 青岛 266000
  • 折叠

摘要

Abstract

Objective To establish a spectrophotometric method for the determination of ferrous iron in ferric chloride hexahydrate. Methods The detection methods on ferrous iron in ferric chloride hexahydrate among European Pharmacopoeia,United States Pharma-copoeia and Chemical Reagent Ferric Chloride Hexahydrate(HG/T3474-2014)of China's Chemical Industry were compared. The last two methods were not easy to operation. On the basis of the European Pharmacopoeia,a method was proposed that after Fe3+ were screened with H3PO4,Fe2+ was measured by spectrophotometry,and the method was verified by experiments. Results and Conclusion The spectrophotometry method is easy to operate and has good reproducibility.

关键词

亚铁离子/六水合三氯化铁/分光光度法/质量控制

Key words

ferrous ion/ferric chloride hexahydrate/spectrophotometry/quality control

分类

医药卫生

引用本文复制引用

白晓光,王正达,邬旭东,段书芬,刘爱华,程晓..六水合三氯化铁中亚铁的检测方法探讨[J].中国药业,2017,26(16):29-31,3.

中国药业

OACSTPCD

1006-4931

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