中国药业2017,Vol.26Issue(16):29-31,3.DOI:10.3969/j.issn.1006-4931.2017.16.009
六水合三氯化铁中亚铁的检测方法探讨
Determination of Ferrous Iron in Ferric Chloride Hexahydrate
白晓光 1王正达 1邬旭东 1段书芬 1刘爱华 1程晓2
作者信息
- 1. 上海拱极化学有限公司,上海 201302
- 2. 青岛国风药业股份有限公司,山东 青岛 266000
- 折叠
摘要
Abstract
Objective To establish a spectrophotometric method for the determination of ferrous iron in ferric chloride hexahydrate. Methods The detection methods on ferrous iron in ferric chloride hexahydrate among European Pharmacopoeia,United States Pharma-copoeia and Chemical Reagent Ferric Chloride Hexahydrate(HG/T3474-2014)of China's Chemical Industry were compared. The last two methods were not easy to operation. On the basis of the European Pharmacopoeia,a method was proposed that after Fe3+ were screened with H3PO4,Fe2+ was measured by spectrophotometry,and the method was verified by experiments. Results and Conclusion The spectrophotometry method is easy to operate and has good reproducibility.关键词
亚铁离子/六水合三氯化铁/分光光度法/质量控制Key words
ferrous ion/ferric chloride hexahydrate/spectrophotometry/quality control分类
医药卫生引用本文复制引用
白晓光,王正达,邬旭东,段书芬,刘爱华,程晓..六水合三氯化铁中亚铁的检测方法探讨[J].中国药业,2017,26(16):29-31,3.