中医药学报2017,Vol.45Issue(3):35-38,4.
GC-MS联用法分析不同产地茅苍术挥发油成分
Analysis on the Volatile Components of Atractylodes Lancea from Different Origins by GC-MS
摘要
Abstract
Objective:To analyze the chemical components of the essential oil extracted from different origins of Atractylodes lancea,and to speculate the fragmentation rules of its main components.Method:The essential oil was extracted by steam distillation and analyzed by GC-MS,and the relative constituent content was calculated with peak area normalization method.The components were finally determined and identified by GC-MS and manual retrieval.Result:Fifty-four components were identified.The fragmentation rules of sesquiterpenes in the essential oil were speculated,i.e.side-chain cleavage before ring-opening.Conclusion:This study provides scientific foundation for the quality control and quality standard of Atractylodes lancea by analyzing its essential oil components and speculating the fragmentation rules of sesquiterpenes.关键词
茅苍术/挥发油/气相色谱-质谱Key words
Atractylodes lancea/Essential oil/GC-MS分类
医药卫生引用本文复制引用
高岩,王知斌,杨春娟,吴高松,陈亚军,匡海学..GC-MS联用法分析不同产地茅苍术挥发油成分[J].中医药学报,2017,45(3):35-38,4.基金项目
教育部博士点基金项目(20132327120002) (20132327120002)
黑龙江中医药大学“优秀创新人才”支持项目(2012RCD05) (2012RCD05)
黑龙江中医药大学“杰出人才培养”基金项目(2012cj02) (2012cj02)