天津科技大学学报2017,Vol.32Issue(4):41-45,62,6.DOI:10.13364/j.issn.1672-6510.20150253
微波辅助酶水解明胶制备多肽酰胺表面活性剂
Preparation of Peptide Amide Surfactant through Microwave Assisted Enzymatic Hydrolysis of Gelatin
摘要
Abstract
Gelatin hydrolysate was prepared through microwave assisted digestion of gelatin using papaya protease.Peptide amide surfactant was synthesized with diethanol amine,gelatin hydrolysate and fatty acid.Raw materials ratio,fatty acid, reaction temperature and reaction time that may affect the properties of the resultant products were studied.The decontami-nation effect and foaming height were investigated.The optimum synthetic conditions were obtained as follows:the hydroly-sis temperature was 55,℃,microwave power was 280,W,and the hydrolysis rate of microwave was 8 times higher thanthat for common enzyme hydrolysis.The best ratio ofm(diethanolamine):m(gelatin hydrolysate):m(lauric acid)is 1:4:1, 145,℃ was selected as the reaction temperature,and the reaction time was 5,h.Under these conditions,PAS has the best surface properties,so it can be applied to the development of skin washing cleaner without water.关键词
多肽酰胺/表面活性剂/水解明胶/皮肤清洗剂Key words
peptide amide/surfactant/gelatin hydrolysate/skin cleaner分类
化学化工引用本文复制引用
吕小凤,律喆,彭啸,吴燕..微波辅助酶水解明胶制备多肽酰胺表面活性剂[J].天津科技大学学报,2017,32(4):41-45,62,6.基金项目
国家自然科学基金资助项目(21107080) (21107080)