中国现代中药2017，Vol.19Issue(7)：929-933,5.DOI:10.13313/j.issn.1673-4890.2017.7.006
HPLC测定蒙药尼安嘎日那格-10中栀子苷的含量
Determination of Geniposide in Mongolian Medicine Ni-Angarinage-10 by HPLC
韩志广 1雷露静 2李旻辉2
作者信息
- 1. 内蒙古自治区赤峰市药品检验所,内蒙古赤峰024000
- 2. 内蒙古自治区中医药研究所,内蒙古呼和浩特010110
- 折叠
摘要
Abstract
Objective:To establish an HPLC method for the determination of geniposide in Mongohan medicine NiAngarinage-10.Methods:The stationary phase was Diamonsil C18 (250 mm ×4.6 mm,5 μm) and the mobile phase was Acetonitrile-Water (11∶89),the flow rate was 1.0 mL · min-1 and the detection wave length was 238 nm.Results:The linear range of geniposide was 6.00 ～ 60.00 μg · mL-1,r =0.999 9.The average recovery was 97.85％ RSD =1.26％.Conclusion:The HPLC method for the determination of geniposide is a simple,fast,accurate and good reproducible.关键词
尼安嘎日那格-10/栀子/栀子苷/HPLCKey words
Ni-Angarinage-10/Fructus Gardeniae/geniposide/HPLC引用本文复制引用
韩志广,雷露静,李旻辉..HPLC测定蒙药尼安嘎日那格-10中栀子苷的含量[J].中国现代中药,2017,19(7):929-933,5.
