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异戊橡胶IR70门尼粘度标准物质的定值

汤妍雯 黄世英 李淑萍

合成材料老化与应用2017,Vol.46Issue(3):70-73,4.
合成材料老化与应用2017,Vol.46Issue(3):70-73,4.

异戊橡胶IR70门尼粘度标准物质的定值

The Fixed Value of Isoprene Rubber(IR 70) Mooney Viscosity Standard Material

汤妍雯 1黄世英 1李淑萍1

作者信息

  • 1. 中国石油兰州化工研究中心国家合成橡胶质量监督检验中心,甘肃兰州730060
  • 折叠

摘要

Abstract

The reference material not only requires sample is uniformity and stability,but also the method of fixed value is right and uncertainty evaluation is reasonable,therefore,the accurate determination and the reasonable evaluation of the uncertainty of the standard material play a crucial role in the development of the standard material.Research group invited 15 laboratories to fix value,analysed the sources of uncertainty and evaluated uncertainty,finally developed isoprene rubber Mooney viscosity (IR 70) standard material.According to the coefficient of skewness and kurtosis coefficient,Grubbs criterion,Cochrane method respectively tested the normal distribution,dubious value,precision of fixed value.These data were in normal distribution,no suspicious,and in equal precision at 95 % confidence probability by test.The nominal value of isoprene rubber (IR 70) was 76.2 ± 1.0 at ML(1 +4)100℃.

关键词

异戊橡胶/门尼粘度/标准物质/定值

Key words

isoprene rubber/Mooney viscosity/standard material/fixed value

分类

化学化工

引用本文复制引用

汤妍雯,黄世英,李淑萍..异戊橡胶IR70门尼粘度标准物质的定值[J].合成材料老化与应用,2017,46(3):70-73,4.

合成材料老化与应用

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1671-5381

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