超高效液相色谱-串联质谱法测定牛尿液中的甲状腺抑制剂OA北大核心CSCDCSTPCD
Determination of thyreostats in bovine urine using ultra-high performance liquid chromatography-tandem mass spectrometry
Five thyreostats (TSs),namely tapazole,thiouracil,methylthiouracil,propylthiouracil,and phenyl-thiouracil,were determined in bovine urine using ultra-high performance liquid chromatography-tandem mass spectrometry (UHPLC-MS/MS ) in positive electrospray ionization mode. Extraction and clean-up were achieved using a ChemElut cartridge with tert-butyl methyl ether,without a derivatization step. Separation was achieved on an Acquity UPLC SS T3 column. The mobil…查看全部>>
Lech RODZIEWICZ;Jolanta MASLOWIECKA;Anna SADOWSKA;Halina CAR
Laboratory of Chemical Examination of Foodstuffs,Department of Veterinary Hygiene,Bialystok 15-959, PolandLaboratory of Chemical Examination of Foodstuffs,Department of Veterinary Hygiene,Bialystok 15-959, PolandDepartment of Experimental Pharmacology,Medical University of Bialystok,Bialystok 15-295,PolandDepartment of Experimental Pharmacology,Medical University of Bialystok,Bialystok 15-295,Poland
化学化工
ultra-high performance liquid chromatography-tandem mass spectrometry (UHPLC-MS/MS )thyreostats (TSs)urine
ultra-high performance liquid chromatography-tandem mass spectrometry (UHPLC-MS/MS )thyreostats (TSs)urine
《色谱》 2017 (10)
1048-1054,7
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