高等学校化学学报2017,Vol.38Issue(10):1709-1718,10.DOI:10.7503/cjcu20170132
Co2+/Dy3+掺杂纳米立方Fe3O4的热还原制备及磁靶向滞留性能
Thermal Reduation Preparation of Co2+/Dy3+Doped Cubic Fe3O4 and Their Magnetic Targeting Retention
摘要
Abstract
Co2+/Dy3+ doped Fe3O4 nanoparticles(MxFe3-xO4) were synthesized by the thermal reduction and co-precipitation methods . The structure, morphology and magnetic properties of Mx Fe3-x O4 were characterized by means of X-ray diffractometer ( XRD ) , transmission electron microscope ( TEM ) and vibrating sample magnetometer(VSM). The results show that the dopants did not change the maternal symmetry, and the mater-nal morphology gradually transformed from cube to sphere. The Mx Fe3-x O4 cubic magnetic particles have maxi-mum saturation magnetization of 7665 and 7021 A · m2 · kg-1 , respectively, when Co2+ actual doping amount is equal to 044 and Dy3+actual doping amount is equal to 005 Compared with the superparamagnet-ic Fe3 O4 , the cubic high magnetic doped Fe3 O4 nanoparticles showed a high retention rate in the simulated magnetic fluid magnetic targeting experiment in vitro.关键词
立方四氧化三铁/掺杂/磁性能/体外模拟磁靶向/晶格常数Key words
Cubic Fe3 O4/Doping/Magnetic property/Magnetic targeting in vitro/Lattice constant分类
化学化工引用本文复制引用
杨宇翔,刘意成,赵敏,袁宏明,姚平平,黄艳,倪超英..Co2+/Dy3+掺杂纳米立方Fe3O4的热还原制备及磁靶向滞留性能[J].高等学校化学学报,2017,38(10):1709-1718,10.基金项目
国家自然科学基金(批准号:20577010, 20971043)资助.Supported by the National Natural Science Foundation of China( Nos. 20577010, 20971043) . (批准号:20577010, 20971043)