中药材2017,Vol.40Issue(3):592-595,4.DOI:10.13863/j.issn1001-4454.2017.03.018
大风子的化学成分研究
Chemical Constituents from the Seeds of Hydnocarpus anthelmintica
摘要
Abstract
Objective:To investigate the chemical constituents of ethyl acetate extract from the seeds of Hydnocarpus anthelmintica.Methods:The chemical constituents were isolated and purified by silica gel,Sephadex LH-20 and other methods,their structures were determined by physicochemical properties and spectroscopic analysis.Results:Thirteen compounds were isolated and identified as 1-acetoxy-4-ethoxy-benzene (1),hydnocarpin (2),luteolin (3),chrysoeriol (4),5-hydroxyindole-3-aldehyde (5),isohydnocarpin(6),trans-coniferyl aldehyde(7),p-hydroxylbenzaldehyde(8),3-hydroxy-4-methoxybenzoic acid(9),syringic acid(10),sinapic aldehyde (11),trans-p-hydroxycinnamic acid (12),2,6-dimethoxy-1,4-benzoquinone (13).Conclusion:Compounds 1,9,11 are isolated from the Hydnocarpus genus for the first time,compounds 1,7,9 ~ 13 are isolated from this plant for the first time,and the 1H-NMR and 13C-NMR data of compound 1 is assigned for the first time.关键词
大风子/化学成分/结构鉴定Key words
Hydnocarpus anthelmintica Pierre./Chemical constituents/Structural determination分类
医药卫生引用本文复制引用
邹欢,张宝,姚成芬,刘俊宏,徐国波,廖尚高,李勇军..大风子的化学成分研究[J].中药材,2017,40(3):592-595,4.基金项目
贵州省科学技术基金项目(20132054) (20132054)
贵州省中药现代化专项项目(20134001) (20134001)
贵州省优青项目(201511) (201511)
贵州省教育厅项目(201304,ZYRC2014012) (201304,ZYRC2014012)
贵州省创新人才团队项目(20165613) (20165613)