中药材2017，Vol.40Issue(3)：600-603,4.DOI:10.13863/j.issn1001-4454.2017.03.020
藏药宽筋藤极性部位的化学成分研究
Chemical Constituents of Tibetan Tinospora sinensis Polar Parts
摘要
Abstract
Objective:To investigate the polar constituents from the herb of Tibetan Tinospora sinensis.Methods:The compounds were isolated and purified by silica gel,semi-preparative HPLC,Sephadex LH-20 and recrystallization methods.Their structures were identified on the basis of spectral analysis and comparison of their spectral date with those in the literature.Results:Twelve compounds were isolated and identified respectively as tinosineside A(1),tinosineside B(2),Cyclo (D-Tyr-D-Tyr)(3),trans-syringin (4),tinoscorside D (5),turpinionoside A (6),3,4-dimethoxyphenyl-O-β-D-apiofuranosyl-(1 →6)-β-D-glucopyranoside (7),3,4,5-trimethoxyphenyl-O-β-D-apiofuranosyl-(1 →6)-β-D-glucopyranoside (8),lcariside F 2 (9),cis-syringin (10),corchoionoside C (11) and pinoresinol(12).Conclusion:Compounds 3,6 ～ 1 1 are isolated from this plant for the first time.关键词
宽筋藤/化学成分/葡萄糖苷/结构鉴定Key words
Tinospora sinensis (Lour.) Merr./Chemical constituent/Glucoside/Structure identification分类
医药卫生引用本文复制引用
白文婷,谢一辉,韦益飞,马亚娟,格桑次仁,黄丽萍..藏药宽筋藤极性部位的化学成分研究[J].中药材,2017,40(3):600-603,4.基金项目
国家自然科学基金委员会地区科学基金项目(81660713) （81660713）
江西民族传统药现代科技与产业发展协同创新中心2014年度协同创新项目(JXXT201402020) （JXXT201402020）
江西中医药大学研究生创新基金(JZYC16529) （JZYC16529）
