中国中医药信息杂志2017，Vol.24Issue(11)：82-85,4.DOI:10.3969/j.issn.1005-5304.2017.11.020
银翘柴黄颗粒质量控制方法研究
Study on Quality Control Method of Yinqiao Chaihuang Granules
摘要
Abstract
Objective To establish the quality control method of Yinqiao Chaihuang Granules.Methods Lonicerae Japonicae Flos, Bupleuri Radix, Scutellariae Radix and Glycyrrhizae Radix et Rhizoma in Yinqiao Chaihuang Granules were identified by TLC, and the content of forsythoside A was detected by HPLC. Results Under the selected chromatographic conditions, TLC spots were clear, the separating was good, and non-interference was found in negative control. Forsythoside A in calibration curve showed good linearity in the range of 0.029 6–0.474 μg, with average recovery of 99.73%, RSD=1.18%. Conclusion The method is accurate and simple, which can be used for the quality control of Yinqiao Chaihuang Granules.关键词
银翘柴黄颗粒/质量控制/薄层色谱法/高效液相色谱法/含量测定Key words
Yinqiao Chaihuang Granules/quality control/TLC/HPLC/content determination分类
医药卫生引用本文复制引用
张丽先,魏悦,王学方,曹静亚,李晓,李自红,李飞飞,李智宁,宁二娟,宋梦娇..银翘柴黄颗粒质量控制方法研究[J].中国中医药信息杂志,2017,24(11):82-85,4.基金项目
河南省科技攻关项目(152102110115) （152102110115）
