分析化学2017，Vol.45Issue(11)：1655-1661,7.DOI:10.11895/j.issn.0253-3820.170333
白蒿挥发油成分的测定及其抗氧化活性分析
Components and Their Antioxidant Activity of Essential Oil of Herba Artimisiae Sieversianae from Different Growth Periods
摘要
Abstract
The effective exploitation of natural products is of great significance. Herein the essential oil from Herba Artimisiae Sieversianae in growth period and flower/ fruit bearing period was extracted by ethanol extraction method. The optimal extraction condition was determined by orthogonal experiment, including extracting 3 times, soaking for 90 min, and the ratios of liquid to solid for Herba Artimisiae Sieversianae in growth period and flower/ fruit bearing period were 10 mL : 1 g and 8 mL : 1 g, respectively. The main components of the products were confirmed by FT-IR and GC-MS, which were cineole, camphor, d-borneol, caryophyllene, cadina-1, 4-diene, calamenene, ethyl palmitate, etc. in herba artimisiae sieversianae in growth period, and camphor, caryophyllene, borneol, neryl formate, etc. in Herba Artimisiae Sieversianae in flower/ fruit bearing period. The radical scavenging activity of the products was determined. The results showed that the IC50 values of the essential oil from Herba Artimisiae Sieversianae in growth period and flower/fruit bearing period for 0. 05 mmol/ L DPPH solution were 0. 40 mg / mL and 1. 66 mg / mL, respectively. The essential oil extracted by ethanol from Herba Artimisiae Sieversianae was confirmed to possess good antioxidant activity.关键词
白蒿挥发油/乙醇浸提法/自由基清除活性Key words
Essential oil of Herba Artimisiae Sieversianae/Ethanol extraction/Radical scavenging activity引用本文复制引用
孙志恒,吕敏兰,张智嘉,张迎,韩晓军..白蒿挥发油成分的测定及其抗氧化活性分析[J].分析化学,2017,45(11):1655-1661,7.基金项目
本文系国家自然科学基金项目( Nos. 21773050, 21528501)、城市水资源与水环境国家重点实验室( 哈尔滨工业大学) 自主课题(No. 2017DX05)和哈尔滨工业大学环境生态创新专项基金项目(No. HSCJ201607)资助 This work was supported by the National Natural Science Foundation of China (Nos. 21773050, 21528501), State Key Laboratory of Urban Water Resource and Environment ( Harbin Institube of Technology) ( No. 2017DX05), and HIT Environment and Ecology Innovation Special Funds (No. HSCJ201617). （ Nos. 21773050, 21528501）
