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《中国药典》方法比较青翘、老翘中连翘苷和连翘酯苷A的含量

胡素连 刘红宇

中医药导报2017,Vol.23Issue(19):41-44,4.
中医药导报2017,Vol.23Issue(19):41-44,4.

《中国药典》方法比较青翘、老翘中连翘苷和连翘酯苷A的含量

To Compare the Content of Phillyrin and Forsythoside A in Green and Grown Fructus Forsythiae with Detection Method in Chinese Pharmacopoeia

胡素连 1刘红宇2

作者信息

  • 1. 湖南中医药大学附属宁乡医院,湖南 长沙410600
  • 2. 湖南中医药大学第一附属医院,湖南 长沙410007
  • 折叠

摘要

Abstract

Objective:To determine the contents of phillyrin and forsythiaside green and grown Fruetus Forsythiae with detection method in Pharmacopoeia,and lay the foundation of further research on its quality standard.Methods:The content of Forsythin (C~H~O11) and Forsythoside A (C29H36O15) was performed by HPLC with wavelength at 277 nm and 330 nm.Results:The linear detection concentration range of phillyrin and forsythiaside was scientific and feasible in 0.22-4.40 μg and 0.108-2.16 μg respectively.The average recovery rate was 100.04% and 98.84%,with RSD was 2.12% and 1.97% respectively.Conclusion:The content of Phillyrin and Forsythoside A had significant difference in green fructus forsythiae and grown fructus forsythiae.

关键词

高效液相法/青翘/老翘/连翘苷/连翘酯苷A

Key words

HPLC/green fructus forsythiae/grown fructus forsythiae/phillyrin/forsythiaside A

分类

医药卫生

引用本文复制引用

胡素连,刘红宇..《中国药典》方法比较青翘、老翘中连翘苷和连翘酯苷A的含量[J].中医药导报,2017,23(19):41-44,4.

基金项目

湖南省中医药科研计划(201574) (201574)

湖南省自然科学基金项目(2006JJ2097) (2006JJ2097)

中医药导报

OACSTPCD

1672-951X

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