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活化木材陶瓷的制备及其孔隙结构表征

孙德林 余先纯 孙德彬 郝晓峰 陈新义 陈美业

中国粉体技术2017,Vol.23Issue(5):13-18,6.
中国粉体技术2017,Vol.23Issue(5):13-18,6.DOI:10.13732/j.issn.1008-5548.2017.05.003

活化木材陶瓷的制备及其孔隙结构表征

Preparation and pore structure characteration of activated woodceramics

孙德林 1余先纯 1孙德彬 1郝晓峰 1陈新义 1陈美业1

作者信息

  • 1. 中南林业科技大学材料科学与工程学院,湖南长沙410004
  • 折叠

摘要

Abstract

Woodceramics which was prepared from pine wood powder and liquefied wood as principal raw materials were activated with KOH as activator,and the low-temperature nitrogen adsorption method and scanning electron microscope (SEM) were employed to survey and observe the effects of activating temperature on the pore structure.The results show that the activating treatment can greatly increase the mesopore and micropore.Its pore structure is a typical H3 type,and most pore diameter distributes in 1.7~2.6 nm,and it still keeps the native pore structure of wood.As the activating temperature raise,the special surface area shows increase at first and then decrease,as well as the pore diameter presents the tendency of decrease at first and then increase.But the activating temperature almost has no effects on the pore diameter of micropore.The special surface area can reach 1 044.0 m2·g-1 as the sample deal with 1 300 ℃ activated temperature and 60 min activated time.

关键词

木材陶瓷/高温活化/孔结构分析

Key words

woodeceramics/high temperature activate/porous structure analysis

分类

机械制造

引用本文复制引用

孙德林,余先纯,孙德彬,郝晓峰,陈新义,陈美业..活化木材陶瓷的制备及其孔隙结构表征[J].中国粉体技术,2017,23(5):13-18,6.

基金项目

国家自然科学基金项目,编号:31670572,31270611. ()

中国粉体技术

OACSCDCSTPCD

1008-5548

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