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溶液法五氯硝基苯单晶生长的研究

王海辉 周新圆 周恒为 黄以能

人工晶体学报2017,Vol.46Issue(10):1936-1940,5.
人工晶体学报2017,Vol.46Issue(10):1936-1940,5.

溶液法五氯硝基苯单晶生长的研究

Study on Growth of PCNB Single Crystals by Solution Method

王海辉 1周新圆 1周恒为 1黄以能2

作者信息

  • 1. 伊犁师范学院物理科学与技术学院,新疆凝聚态相变与微结构实验室,伊宁835000
  • 2. 南京大学物理学院,国家固体微结构重点实验室,南京 210093
  • 折叠

摘要

Abstract

Solubility of PCNB was determined in acetone solvent .The PCNB single crystals were successfully grown by constant temperature solvent evaporation method in acetone for the first time .The results show that:there is a smaller temperature coefficient zone below 302 K, which is suitable for the growth of single crystals by constant temperature evaporation method;the PCNB single crystals with centimeter size were obtained;the IR and Raman spectra show that the crystals have not incorporated solvent;XRD analysis indicates that the lattice structure of PCNB crystals is hexagonal and have good quality .

关键词

PCNB/溶解度/晶体生长

Key words

PCNB/solubility/crystal growth

分类

数理科学

引用本文复制引用

王海辉,周新圆,周恒为,黄以能..溶液法五氯硝基苯单晶生长的研究[J].人工晶体学报,2017,46(10):1936-1940,5.

基金项目

新疆维吾尔自治区科技创新团队培养建设项目(2014751001) (2014751001)

国家自然科学基金(11664042) (11664042)

伊犁师范学院2016 年新疆维吾尔自治区自治区级大学生创新创业训练计划(201610764024) (201610764024)

人工晶体学报

OA北大核心CSCDCSTPCD

1000-985X

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