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改进共沉淀法制备SrMoO4:Eu3+荧光粉及其荧光性能研究

何晓燕 张涛 穆冬迪 欧阳艳

人工晶体学报2017,Vol.46Issue(10):2025-2029,5.
人工晶体学报2017,Vol.46Issue(10):2025-2029,5.

改进共沉淀法制备SrMoO4:Eu3+荧光粉及其荧光性能研究

Preparation and Fluorescence Properties of SrMoO4:Eu3+Phosphor by Modified Co-precipitation Method

何晓燕 1张涛 1穆冬迪 2欧阳艳1

作者信息

  • 1. 伊犁师范学院化学与环境科学学院,伊宁 835000
  • 2. 伊犁师范学院凝聚态相变与微结构重点实验室,伊宁835000
  • 折叠

摘要

Abstract

A series of SrMoO 4 :Eu3 +red fluorescent materials were synthesized by the improved coprecipitation method and the addition of modifier .The synthesized samples were characterized by X-ray powder diffraction (XRD), scanning electron microscopy (SEM), and fluorescence spectrophotometer ( PL ) . The relationship between the fluorescence properties and the types of modifiers , modifier addition , reactant concentration and activation of ion doping and other reaction parameters was explored . The results show that SrMoO 4:Eu3+has four groups of Eu 3+ion excitation peaks at 420-750 nm under the excitation of excitation light at a wavelength of 271 nm, and the strongest peak emits red light at 616 nm. The fluorescence performance was the best when the addition was 3 mL polyethylene glycol ( PEG) .With the increase of Eu 3+doping amount , the characteristic emission peak at 616 nm shows the first increase and then decreases .When the Eu 3+doping amount is 11%, the maximum value is reached .Emission intensity of Eu3+doped SrMoO4 phosphor at 616 nm is the strongest, indicating that SrMoO4:Eu3+is a kind of red fluorescent material which can be applied to white LED .

关键词

SrMoO4:Eu3+/改进共沉淀法/红色荧光粉/荧光性能

Key words

SrMoO4:Eu3+/improved coprecipitation method/red phosphor/fluorescence property

分类

数理科学

引用本文复制引用

何晓燕,张涛,穆冬迪,欧阳艳..改进共沉淀法制备SrMoO4:Eu3+荧光粉及其荧光性能研究[J].人工晶体学报,2017,46(10):2025-2029,5.

基金项目

新疆维吾尔自治区高校科研计划重点项目(XJEDU2016I044) (XJEDU2016I044)

自治区研究生科研创新项目(XJGRI2016137) (XJGRI2016137)

人工晶体学报

OA北大核心CSCDCSTPCD

1000-985X

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