现代科学仪器Issue(4):123-126,4.
多目标区域地球化学调查样品中汞的测定
Determination of Hg in Samples of Multi-purpose Regional Geochemical Survey
邹国庆 1方超 1王小云1
作者信息
- 1. 中国冶金地质总局第一地质勘察院测试中心 河北三河065201
- 折叠
摘要
Abstract
It is difficult to meet the detection limit of "the specification of multi-purpose regional geochemical survey (1∶ 2500000)" for Hg in the samples.The cold atomic fluorescence spectrometry was chosen to analyze the Hg element concentration of the samples.The working conditions such as lamp current,negative pressure,carrier gas flow and atomization temperature was optimized.The results showed optimized method meets the analysis method requirement of "the specification of multi-purpose regional geochemical survey (1∶ 2500000)".The Method detection limit is 0.19 ng/g.The △lgC (n =12) ofGBW07301a,GBW07428 and GBW07426 is 0.000,0.030 and 0.043,respectively.The RSD (n =12) of the three standard materials is 4.95% and 4.33%,6.98%,respectively.关键词
多目标区域地球化学调查/原子荧光光谱/汞/检出限Key words
Multi-purpose regional geochemical survey/Atomic fluorescence spectrometry/Hg/Determination limit分类
天文与地球科学引用本文复制引用
邹国庆,方超,王小云..多目标区域地球化学调查样品中汞的测定[J].现代科学仪器,2017,(4):123-126,4.