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紫外荧光法分析工业芳烃中痕量硫

许竞早 王川 彭振磊 张育红

石油化工2017,Vol.46Issue(11):1419-1423,5.
石油化工2017,Vol.46Issue(11):1419-1423,5.DOI:10.3969/j.issn.1000-8144.2017.11.013

紫外荧光法分析工业芳烃中痕量硫

Analysis of trace sulfur in aromatic hydrocarbon by ultraviolet fluorescence

许竞早 1王川 1彭振磊 1张育红1

作者信息

  • 1. 中国石化 上海石油化工研究院,上海 201208
  • 折叠

摘要

Abstract

A ultraviolet fluorescence method for the analysis of trace sulfur in aromatic hydrocarbon was established. The method was applicable to industrial aromatic content of sulfur. In order to ensure the accurate detection of trace sulfur,the operation conditions of the instrument were optimized and a series of control measures were established. The sulfide had a good linear relationship with its mass 2.0×10-9-5.0×10-8 g,the correlation coefficient was 0.9988. The recoveries of the sulfur content in aromatic hydrocarbon were 94.55%-116.67%,the relative standard deviations were 2.09%-9.23%. The limits of detection were 0.018 mg/kg. This method can applied to the determination of trace sulfur in aromatic hydrocarbon.

关键词

紫外荧光法/痕量硫/芳烃/分析

Key words

ultraviolet fluorescence/trace sulfur/aromatic hydrocarbon/analysis

分类

能源科技

引用本文复制引用

许竞早,王川,彭振磊,张育红..紫外荧光法分析工业芳烃中痕量硫[J].石油化工,2017,46(11):1419-1423,5.

石油化工

OA北大核心CSCDCSTPCD

1000-8144

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