大学化学2017，Vol.32Issue(12)：53-59,7.DOI:10.3866/PKU.DXHX201704010
8-羟基喹啉及其铝配合物的合成、表征及发光性能——推荐一个综合化学实验
Synthesis,Characterization and Luminescence Properties of 8-Hydroxyquinoline and Tris(8-hydroxyquinolinato)Aluminum:A Comprehensive Chemistry Experiment
摘要
Abstract
First, 8- hydroxyquinoline(HQ) was synthesized by the Skraup method, which involves basic skills of organic chemistry experiment such as reflux heating, steam distillation, crystallization and recrystallization. Secondly, the synthesized 8-hydroxyquinoline was used to prepare AlQ3 in which Al content was measured by back titration. Finally, infrared spectra, hydrogen nuclear magnetic resonance spectra, UV-Vis absorption spectra and fluorescence emission spectra of 8-hydroxyquinoline as well as AlQ3 were measured. This experiment covers synthesis,characterization and performance testing, facilitating students to understand and complete a basic research process.关键词
三(8-羟基喹啉)合铝/发光/综合化学实验Key words
Tris(8-hydroxyquinolinato)aluminum/Luminescence/Comprehensive chemistry experiment分类
社会科学引用本文复制引用
王周,石建新,彭敏,郑赛利,赖瑢,李莲云,陈六平..8-羟基喹啉及其铝配合物的合成、表征及发光性能——推荐一个综合化学实验[J].大学化学,2017,32(12):53-59,7.基金项目
2017年中山大学校级质量工程项目"重点教材建设项目" （）
