中药材2017，Vol.40Issue(7)：1595-1599,5.DOI:10.13863/j.issn1001-4454.2017.07.020
牛尾菜根茎的化学成分研究
Chemical Constituents from Roots of Smilax riparia
摘要
Abstract
Objective:To investigate the chemical constituents of roots from Smilax riparia.Methods:The column chromatography and high performance liquid chromatogarphy(HPLC) were used to isolate and purify the cotnpounds of n-butanol and ethyl acetate extract of Smilax riparia.The chemical structures were identified on basis of physic-chemical properties and spectral data.Results:18 compounds were isolated and identified as erythro-4',5',7,9,9'-pentahydroxy-3-methoxy-8-O-4′-neolignan-3′-O-fβ-glucopyranoside (1),smilaside A (2),(7S,8S)-3-methoxyl-3'-O-β-D-glucopyrannosyl-4',8,5',7-diepoxyneolignan-4,9 ′-diol (3),umbelliferone (4),phlorigidoside B (5),7-O-methyl-10-oxy-thymol gentiobioside (6),norartocarpetin (7),diosmetin (8),lirioresinol-B-dimethyl ether (9),(+)-syringaresinol-4-O-β-D-glucopyranosyl-(1 →6)-β-D-glucopyranoside (10),(+)-pinoresinol4-O-β-D-glucopyranosyl-(1 →6)-β-D-glucopyranoside (11),syringin (12),benzoic acid (13),4-hydroxybenzoic acid (14),p-hydroxycinnamic (15),isovanilli acid (16),phydroxybenzaldehyde(17)and 3,4-dihydroxybenzaldehyde(18).Conclusion:Compounds 1 ～12 are isolated from this plant for the first time.关键词
牛尾菜/化学成分/结构鉴定Key words
Smilax riparia A.DC./Chemical constituents/Structure identification分类
医药卫生引用本文复制引用
龚韦凡,邹大江,高瑞锡,黄先菊,杨光忠,李竣..牛尾菜根茎的化学成分研究[J].中药材,2017,40(7):1595-1599,5.基金项目
湖北省高等学校优秀中青年科技创新团队计划资助项目(T201220) （T201220）
中央高校基本科研业务费专项资金项目(3212015CZW15029,YCZW15095) （3212015CZW15029,YCZW15095）
中南民族大学实验室开放与技改资助项目(KF2016005,JG2016004) （KF2016005,JG2016004）
