中国现代中药2017，Vol.19Issue(10)：1454-1460,7.DOI:10.13313/j.issn.1673-4890.2017.10.021
蒙药漆树膏的炮制工艺及质量标准研究
Study on Processing Technology and Quality Standard of Mongolian Medicine Qishugao
摘要
Abstract
Objective:To establish the processing standard of Mongolian medicine Qishugao.Methods:According to literature,the representative processing method was selected,and optimized through orthogonal design.Referring to the China Pharmacopoeia (2015),the relevant method was used to identify phenols,and measure water content,ash content and ethanolic extract.The total phenol as active component was detected with gallic acid as reference substance by spectrometric method.Results:The optimal preparation for Qishugao was butter cream processing,the condition was as follows:drug and butter ratio 1∶3,butter the surface temperature 200 ℃,soaking time 20 min.The color reaction of ferric chloride was positive.The water content of the three batches was between 6.59％-11.28％.The total ash content was between 3.02％-7.55％.The content of acid-insoluble ash was between 1.15％-4.49％.The content of alcohol soluble extract was between 9.55％-22.97％.The total phenol content was 0.182-1.254 mg ·L-1.The average recovery was 99.31％,RSD was 1.55％,and the total phenol content was between 10.34-20.45 mg ·g-1.Conclusion:The processing method is consistent with modern technology,it also follows traditional Mongolian medicine experience.关键词
蒙药/漆树膏/没食子酸/总酚/紫外分光光度法/质量标准Key words
Mongolian medicine/Qishugao/gallic acid/total phenols/UV/quality standard引用本文复制引用
包勒朝鲁,吴·斯琴毕力格,那生桑,乌兰图雅..蒙药漆树膏的炮制工艺及质量标准研究[J].中国现代中药,2017,19(10):1454-1460,7.基金项目
内蒙古自治区科技计划项目(20151230) （20151230）
