医药导报2018，Vol.37Issue(2)：219-222,4.DOI:10.3870/j.issn.1004-0781.2018.02.019
盐杜仲配方颗粒的质量标准
Quality Standards of Salt Eucommia Dispensing Granules
摘要
Abstract
Objective To establish the quality standards for salt eucommia dispensing granules. Methods The extractives were obtained by alcohol extraction method. HPLC was applied for the determination of pinoresinol diglucoside in dispensing granules. HPLC fingerprints were established by the contrast of Agilent 1260 HPLC, Waters HPLC and various chromatogram column. Results Pinoresinol diglucoside showed a good linear relationship ( Y = 2. 9594X + 3. 2825,R2 =0.9999) at 102.8-2056.0 mg?L-1 with average recovery of 99.85％ (RSD = 0.31％,n = 9). Conclusion The method is easy-operated and accurate,which has a good specificity for the quality control of common salt eucommia dispensing granules.关键词
盐杜仲/配方颗粒/质量标准/松脂醇二葡萄糖苷/色谱法,高效液相Key words
Salt eucommia/Dispensing granules/Quality standards/Pinoresinol diglucoside/Chromatography,high performance liquid分类
医药卫生引用本文复制引用
胡辉,龙林,刘重阳,李先芝,梅之南..盐杜仲配方颗粒的质量标准[J].医药导报,2018,37(2):219-222,4.基金项目
2016年湖北省技术创新专项重大项目(2016ACA142) （2016ACA142）
