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汉中不同规格延胡索质量评价

王晓婷 王亚恒 王芳 王昌利 王小平 白吉庆

中国现代中药2017,Vol.19Issue(11):1578-1581,4.
中国现代中药2017,Vol.19Issue(11):1578-1581,4.DOI:10.13313/j.issn.1673-4890.2017.11.017

汉中不同规格延胡索质量评价

Quality Evaluation of Corydalis Tuber in Different Specifications in Hanzhong

王晓婷 1王亚恒 2王芳 1王昌利 1王小平 1白吉庆2

作者信息

  • 1. 陕西中医药大学,陕西咸阳712046
  • 2. 陕西省中药原料质量监测技术服务中心,陕西咸阳712046
  • 折叠

摘要

Abstract

Objective:To investigate the quality difference of Corydalis tuber planting years and its annual large and small size of corydalis.Methods:Tetrahydropalmatine in each sample was determined by HPLC with Dima C18 column (250 mm × 4.6 mm,5 μm),mobile phase of methanol-0.1% phosphoric acid solution (triethylamine adjusted to pH 6) =67∶33,the flow rate of 1 mL · min-1,column temperature of 30 ℃ and detection wavelength of 280 nm.Results:Comparison of the content of Corydalis tuber in different years,the drying rate was the highest in the annual small tubers and tetrahydropalmatine content reached to 1.776 9 mg ·g-1,while the drying rate was the lowest for biennial tubers,and tetrahydropalmatine was 1.537 4 mg ·g-1.Conclusion:There are differences in the quality of different Corydalis tuber with different growth years and annual sizes.

关键词

延胡索/延胡索乙素/高效液相色谱法/含量测定

Key words

Corydalis Rhizoma/tetrahydropalmatine/HPLC/determination of content

引用本文复制引用

王晓婷,王亚恒,王芳,王昌利,王小平,白吉庆..汉中不同规格延胡索质量评价[J].中国现代中药,2017,19(11):1578-1581,4.

基金项目

2015年中医药部门公共卫生服务补助资金项目(国中医药发规财[2015]21号) (国中医药发规财[2015]21号)

中国现代中药

OACSTPCD

1673-4890

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