中国现代中药2017，Vol.19Issue(12)：1754-1757,4.DOI:10.13313/j.issn.1673-4890.2017.12.020
八珍益母丸中芍药苷的HPLC法测定结果的不确定度评价
Uncertainty Evaluation on Paeoniflorin Content Determination of Bazhen Yimu Pills by HPLC
马晓静 1崔业波 1高楠楠1
作者信息
- 1. 四平市食品药品检验所,吉林 四平136000
- 折叠
摘要
Abstract
Objective:To analyze the uncertainty of determination of paeoniflorin in Bazhen Yimu Pillls by HPLC and find out the effect factors of uncertainty.Methods:The content determination method for Bazhen Yimu Pills in Chinese Pharmacopoeia(CP)2015 was applied for the study.The determination process and procedures were analyzed,and the combined uncertainty was calculated and finally the extended uncertainty were obtained in 95％ confidence intervals.Results:The expanded uncertainty for the HPLC determination of paeoniflorin is 0.20 mg in each pill.Conclusion:The uncertainty of the experiment is mainly caused by the weight of standard,strict control of the weighing process will help to improve reliability and accuracy of test results.关键词
八珍益母丸/芍药苷/含量测定/不确定度/高效液相色谱法Key words
Bazhen Yimu Pills/paeoniflorin/content determination/uncertainty/HPLC引用本文复制引用
马晓静,崔业波,高楠楠..八珍益母丸中芍药苷的HPLC法测定结果的不确定度评价[J].中国现代中药,2017,19(12):1754-1757,4.
