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3种人工结香方法所得沉香挥发性成分的SPME/GC-MS分析

张静斐 吴惠勤 黄晓兰 林晓珊 马艳芳 侯思润

分析测试学报2018,Vol.37Issue(1):10-16,7.
分析测试学报2018,Vol.37Issue(1):10-16,7.DOI:10.3969/j.issn.1004-4957.2018.01.002

3种人工结香方法所得沉香挥发性成分的SPME/GC-MS分析

SPME/GC-MS Analysis on Volatile Constituents of Agarwood Produced by Three Artificial Inducing Methods

张静斐 1吴惠勤 2黄晓兰 3林晓珊 1马艳芳 1侯思润1

作者信息

  • 1. 广东省测试分析研究所,广东省分析测试技术公共实验室,广东广州510070
  • 2. 中国科学院广州化学研究所,广东广州510650
  • 3. 中国科学院大学,北京100049
  • 折叠

摘要

Abstract

The volatile compositions of agarwood were produced by biological,chemical and physical (flame drilled) methods,then enriched by solid phase microextraction and isolated and identified by GC-MS.The quality of the agarwood produced was evaluated.Investigation showed that the volatile compositions of the agarwood were all composed of sesquiterpenoids and aromatic compounds,but the chemical compositions and contents of the agarwood were quite different because of the different artificial inducing methods.The six characteristic components,i.e.agarofuran,hinesol,4-phenyl-2-butanone,p-methoxybenzylacetone,agarospirol and baimuxinal,and their contents were used as the evaluation indexes for the agarwood quality.The content of agarospirol in the flame drilled agarwood was the highest,which was about 5.5%.The total content of characteristic components in the agarwood produced by biological method was the highest,which reached to 16.6%,followed by that of the flame drilled agarwood,which was around 13.6%,and the agarwood produced by chemical method was the lowest.The result showed the biological method has the best agarwood quality,the flame drilled method was slightly poor,and they were both superior to the chemical method.

关键词

沉香/固相微萃取/气相色谱-质谱联用/挥发性成分/结香方法

Key words

agarwood/SPME/GC-MS/volatile constituents/artificial inducing methods

分类

化学化工

引用本文复制引用

张静斐,吴惠勤,黄晓兰,林晓珊,马艳芳,侯思润..3种人工结香方法所得沉香挥发性成分的SPME/GC-MS分析[J].分析测试学报,2018,37(1):10-16,7.

基金项目

广东省科技计划项目(2016A040403063) (2016A040403063)

分析测试学报

OA北大核心CSCDCSTPCD

1004-4957

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