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ICP-MS法测定壮药了刁竹中5种重金属元素的含量

陈松 黄必奎 黄瑞松 覃思苗

广西医科大学学报2018,Vol.35Issue(1):10-13,4.
广西医科大学学报2018,Vol.35Issue(1):10-13,4.DOI:10.16190/j.cnki.45-1211/r.2018.01.003

ICP-MS法测定壮药了刁竹中5种重金属元素的含量

Determination of five elements in Zhuang medicine Cynanchum Paniculatum (Bunge) Kitagawa by ICP-MS

陈松 1黄必奎 1黄瑞松 2覃思苗1

作者信息

  • 1. 广西壮族自治区百色食品药品检验所,百色533000
  • 2. 广西壮族自治区民族医药研究院,南宁530001
  • 折叠

摘要

Abstract

Objective:To quantify the contents of heavy metal elements in Zhuang medicine Cynanchum Paniculatum (Bunge) Kitagawa from different areas,and to understand its heavy metal pollution.Methods:Determination ofPb,Cd,As,Hg,Cu contents in C.Paniculatum (Bunge) Kitagawa by ICP-MS with internal standard calibration and quantitative analysis.Cu and As used Sc as internal standard,Cd used In as internal standard,Pb and Hg used Bi as internal standard.Results:The total content of each element in the 10 samples of C.Paniculatum (Bunge) Kitagawa from different areas were detected,content range of each element were:Pb 0.2301-0.6836 mg/kg,Cd 0.0717-0.1957 mg/kg,As 0.0250-0.0750 mg/kg,Hg 4.2794-7.7946 μg/ kg,Cu 0.9943-1.5444 mg/kg.Conclusion:10 batches of samples were detected a certain amount of heavy metals,but the content did not exceed the Chinese Pharmacopoeia 2015 version of a Chinese herbal medicine related provisions of the limit.

关键词

壮药/了刁竹/ICP-MS/重金属含量

Key words

Zhuang medicine/Cynanchum Paniculatum (Bunge) Kitagawa/ICP-MS/heavy metal content

分类

医药卫生

引用本文复制引用

陈松,黄必奎,黄瑞松,覃思苗..ICP-MS法测定壮药了刁竹中5种重金属元素的含量[J].广西医科大学学报,2018,35(1):10-13,4.

基金项目

广西科技厅重大专项计划项目(No.桂科重1355001-4-2) (No.桂科重1355001-4-2)

广西食品药品监督管理局广西壮药质量标准(第三卷)质量评价与标准研究项目(No.GXZC2014-G3-1577-YLZB-B-2) (第三卷)

广西卫生厅重点科研课题(No.重2012015) (No.重2012015)

广西医科大学学报

OACSTPCD

1005-930X

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