中国现代中药2017,Vol.19Issue(9):1305-1310,6.DOI:10.13313/j.issn.1673-4890.2017.9.019
补肾蠲毒丸质量标准研究
Study on Quality Standard of BushenJuandu Pills
摘要
Abstract
Objective:To establish the quality standard for Bushen Juandu Pills.Methods:The Dioscoreae Rhizoma,Sophorae Flavescentis Radix,Bombyx Batryticatus and Curcumae Radix were identified by microscopic identification.The Cuscutae Semen,Polygoni Cuspidati Rhizoma et Rradix,Scutellariae Radix and Paeoniae Radix Rubra were identified by TLC,and the content of astragaloside was determined by HPLC-ELSD.Results:The microscopic characteristics were obvious,TLC spots were clear and strong specific.In the content determination method,astragaloside showed a good linear relationship at the range of 0.252 0-3.150 0 μg,r =0.999 6.The average recovery rate was 99.80%.Conclusion:The established method is accurate and reliable and easy to operate,it can be used for the quality control of Bushen Juandu pills.关键词
补肾蠲毒丸/质量标准/显微鉴别/薄层色谱法/高效液相色谱-蒸发光散射检测法Key words
Bushen Juandu Pills/quality standard/microscopic identification/TLC/HPLC-ELSD引用本文复制引用
盛晓静,周鹤,赖杰仁..补肾蠲毒丸质量标准研究[J].中国现代中药,2017,19(9):1305-1310,6.基金项目
九江市社会发展与软科学类科研计划项目(九科字[2015]44号-20) (九科字[2015]44号-20)