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补肾蠲毒丸质量标准研究

盛晓静 周鹤 赖杰仁

中国现代中药2017,Vol.19Issue(9):1305-1310,6.
中国现代中药2017,Vol.19Issue(9):1305-1310,6.DOI:10.13313/j.issn.1673-4890.2017.9.019

补肾蠲毒丸质量标准研究

Study on Quality Standard of BushenJuandu Pills

盛晓静 1周鹤 1赖杰仁2

作者信息

  • 1. 九江市食品药品检验所,江西九江332000
  • 2. 九江市中医医院,江西九江332000
  • 折叠

摘要

Abstract

Objective:To establish the quality standard for Bushen Juandu Pills.Methods:The Dioscoreae Rhizoma,Sophorae Flavescentis Radix,Bombyx Batryticatus and Curcumae Radix were identified by microscopic identification.The Cuscutae Semen,Polygoni Cuspidati Rhizoma et Rradix,Scutellariae Radix and Paeoniae Radix Rubra were identified by TLC,and the content of astragaloside was determined by HPLC-ELSD.Results:The microscopic characteristics were obvious,TLC spots were clear and strong specific.In the content determination method,astragaloside showed a good linear relationship at the range of 0.252 0-3.150 0 μg,r =0.999 6.The average recovery rate was 99.80%.Conclusion:The established method is accurate and reliable and easy to operate,it can be used for the quality control of Bushen Juandu pills.

关键词

补肾蠲毒丸/质量标准/显微鉴别/薄层色谱法/高效液相色谱-蒸发光散射检测法

Key words

Bushen Juandu Pills/quality standard/microscopic identification/TLC/HPLC-ELSD

引用本文复制引用

盛晓静,周鹤,赖杰仁..补肾蠲毒丸质量标准研究[J].中国现代中药,2017,19(9):1305-1310,6.

基金项目

九江市社会发展与软科学类科研计划项目(九科字[2015]44号-20) (九科字[2015]44号-20)

中国现代中药

OACSTPCD

1673-4890

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