大学化学2018，Vol.33Issue(1)：69-72,4.DOI:10.3866/PKU.DXHX201707014
5-甲氧基-2-苯基-2,3-二氢苯并呋喃的制备——介绍一个大学综合化学实验
Preparation of 5-Methoxy-2-PhenyI-2,3-Dihydrobenzofuran: A Comprehensive CoIIege Chemistry Experiment
摘要
Abstract
A new comprehensive college chemistry experiment was introduced. 5-Methoxy-2-phenyl-2,3-dihydrobenzofuran was prepared from 4-methoxyphenol and styrene by using 1,1,1,3,3,3-hexafluoropropan-2-ol as the solvent and 2,3-dichloro-5,6-dicyanobenzoquinone as the oxidant at room temperature. The structure was identified by IR, 1H NMR, 13C NMR and HRMS. In the experiment, students' research interest and exploring spirit will be stimulated, the skill of comprehensive experiment operation and analysis will be improved, and furthermore, the innovative thinking and scientific research ability will be cultivated.关键词
5-甲氧基-2-苯基-2,3-二氢苯并呋喃/对甲氧基苯酚/苯乙烯Key words
5-Methoxy-2-phenyl-2/3-dihydrobenzofuran/4-Methoxy-phenol/Styrene分类
社会科学引用本文复制引用
王云侠,赵宇,王兰英,李剑利..5-甲氧基-2-苯基-2,3-二氢苯并呋喃的制备——介绍一个大学综合化学实验[J].大学化学,2018,33(1):69-72,4.基金项目
西北大学质量与教学改革工程项目(JX14046) （JX14046）
陕西省科技计划项目(2017KW-066) （2017KW-066）
西安市科技计划项目 （）
西北大学合成与天然功能分子化学教育部重点实验室开放基金 （）
