石油化工2018，Vol.47Issue(2)：175-180,6.DOI:10.3969/j.issn.1000-8144.2018.02.011
一种铝交联压裂液稠化剂的合成与评价
Synthesis and evaluation of a thickener of fracturing fluid crosslinked by aluminum compound
刘通义 1唐瑭 1戴秀兰 2魏俊 2陈光杰2
作者信息
- 1. 西南石油大学 化学化工学院,四川 成都 610500
- 2. 成都佰椿石油科技有限公司,四川 成都 610500
- 折叠
摘要
Abstract
A fracturing fluid thickener(CTMA),was prepared by using aqueous solution copolymerization with acrylamide(AM),N-methylolacrylamide(NMA)and hydrophobic cationic(CT1) as monomer and potassium persulfate and sodium sulfite as initiator. The structure of CTMA was characterized by FTIR and its dissolving ability,thickening ability,water insoluble matter content,residue quantity, suspended sand performance and shearing and temperature resistance were evaluated. Characterization results indicated that the polymerization took place among the monomers and the structure of synthesized CTMA coincided with the target structure. The results showed that the optimal reaction temperature was 33 ℃;the dosage of initiator was 0.2%(w) of total mass of monomers;the ratio of monomers was m(AM):m(NMA):m(CT1)=100:0.1:0.05;the optimal volume ratio of polymer solution to crosslinker was 2%(φ) and when the pH value of gelling is 3 the crosslinked gel can achieve the best hanging ability. CTMA has good dissolving and thickening ability and is low in water insoluble matter content and residue quantity. The formed fracturing fluid has stable suspended sand performance and excellent shearing and temperature resistance.关键词
压裂液/稠化剂/铝交联Key words
fracturing fluid/thickener/aluminum crosslinking分类
化学化工引用本文复制引用
刘通义,唐瑭,戴秀兰,魏俊,陈光杰..一种铝交联压裂液稠化剂的合成与评价[J].石油化工,2018,47(2):175-180,6.
