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棕榈油基钻井液降滤失剂的研制

张瑞 徐加放 顾甜甜 丁廷稷 于政廉 李力文 罗海

钻井液与完井液2017,Vol.34Issue(6):29-34,6.
钻井液与完井液2017,Vol.34Issue(6):29-34,6.DOI:10.3969/j.issn.1001-5620.2017.06.006

棕榈油基钻井液降滤失剂的研制

Development of a Filter Loss Reducer for Palm Oil Base Drilling Fluid

张瑞 1徐加放 1顾甜甜 1丁廷稷 1于政廉 1李力文 1罗海1

作者信息

  • 1. 中国石油大学(华东)石油工程学院·海洋水下设备试验与检测技术国家工程实验室,山东青岛266580
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摘要

Abstract

Palm oil has the advantages of good biodegradability,low cost and being environmentally friendly.It can be used as the base fluid of oil base drilling fluid.Palm oil has different components and molecular structures than those of diesel oil and white oil,and filter loss reducers presently available for use in conventional oil base drilling fluids cannot be used in palm oil base drilling fluid,and it is thus necessary to develop filter loss reducers special for use in palm oil base drilling fluid.Dry method,wet method and chloroformylation reaction were used to prepare and optimize filter loss reducers for palm oil base drilling fluid.Evaluation of the performance of the optimized filter loss reducer indicated that a filter loss reducer FLA made from SAA-6 (an organic modifying agent) and sodium humate through ionic adsorption reaction (wet method) had the best performance.FLA had colloidal coefficient of 92% in palm oil drilling fluid,and the optimum reaction conditions for the production of FLA was 95 ℃,2 h of reaction time,and ratio of sodium humate to SAA-6 of 5.5.A palm oil drilling fluid treated with 5% FLA had API filtration rate of less than 4 mL and yield point of about 8 Pa,demonstrating good filtration behavior.The FLA treated palm oil drilling fluid had good thermal stability;it functioned properly at 150 ℃,and had HTHP filter loss of less than 9 mL.Laboratory experiments showed that this drilling fluid had inhibitive capacity,lubricity,contamination resistance,reservoir protective capacity and bio-toxicity that all satisfied the needs of drilling operations.This study provides an experimental base for the application of palm oil in drilling fluids.

关键词

油基钻井液/棕榈油/降滤失剂/腐植酸钠/有机改性剂/环境保护

Key words

Drilling fluid/Filter loss reducer/Sodium humate/Filter loss reduction/Organic modifying agent/Palm oil

分类

能源科技

引用本文复制引用

张瑞,徐加放,顾甜甜,丁廷稷,于政廉,李力文,罗海..棕榈油基钻井液降滤失剂的研制[J].钻井液与完井液,2017,34(6):29-34,6.

基金项目

973项目“海洋深水油气安全高效钻完井基础研究”(2015CB251200),国家重点研发计划“极地冰区钻井防寒工艺技术研究”(2016YFC0303408). (2015CB251200)

钻井液与完井液

OA北大核心CSTPCD

1001-5620

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