热带作物学报2017,Vol.38Issue(12):2382-2387,6.DOI:10.3969/j.issn.1000-2561.2017.12.028
芥末精油-β-环糊精包合物制备工艺、微结构及缓释特性研究
Preparation Process of Mustard Essential Oil-β-Cylcodextrin Inclusion Complex and Characterization of Microstructure and Release Properties
摘要
Abstract
The preparation process,microstructure and release characteristics of mustard essential oil-β-cyclodextrin inclusion were studied.Firstly,the optimization of the preparation process was conducted with the guide of inclusion rate and product yield,based on the single factor and orthogonal experimental design;Secondly,the micro-structure was observed by scanning electron microscopy while release properties were studied under controlled temperatures and humidity.The optimum condition of inclusion process was as follows:1∶6 (ratio of mustard oil and cyclodextrin inclusion ratio),1.5 h (inclusion time) and 50 ℃ (inclusion temperature).The process could achieve inclusion rate of 90.56% and product yield of 87.22%.Results of scanning electron microscopy showed that the inclusion complex appears uniform and irregular in shape.Release rates of essential oil were directly correlated with relative humidity and temperature.关键词
芥末精油/环糊精/包合物/缓释Key words
Mustard essential oil/cylcodextrin/inclusion complex/controlled release分类
轻工纺织引用本文复制引用
李奕星,李芬芳,陈娇,袁德保..芥末精油-β-环糊精包合物制备工艺、微结构及缓释特性研究[J].热带作物学报,2017,38(12):2382-2387,6.基金项目
海南省自然科学基金面上项目(No.20163097) (No.20163097)
中国热带农业科学院院本级基本科研业务员费专项资金(No.1630052015046) (No.1630052015046)
海南省社会发展科技专项(No.2015SF34) (No.2015SF34)
中央级公益性科研院所基本科研业务费专项-中国热带农业科学院院级创新团队项目(No.17CXTD-20). (No.17CXTD-20)